Project Description

Good producer 100-66-3 superior manufacturer Anisole

Description

  • Brand:乐动体育最新版本

  • Product Name:Anisole

  • Synonyms:Methoxybenzine;Anisole, SuperDry, J&KSeal;Benzene,methoxy-;Ether, methyl phenyl-;ether,methylphenyl;femanumber:2097;methoxy-benzen;Phenoxymethane

  • CAS No.:100-66-3

  • MF:C7H8O

  • MW:108.14

  • Packaging:200kg/Plastic drum,or according to the requirements of the customers

What is the use ofAnisole

1. Mainly used for brewing wine flavor, fennel and fennel.
2. Wood analysis reagents and solvents, also used in the preparation of spices and intestinal pesticides
3. Used in the production of spices, dyes, medicines, pesticides, and solvents
4. Used in organic synthesis, as well as furniture, perfume and insect repellent.
5. Solvents for automobile recrystallization, controller fillers, refractive index measurement, spices, organic synthesis intermediates

Pipe products

AnisoleSpecification

Appearance Transparent colorless liquid
Purity 99.5%min
Melting point ‘-37 °C (lit.)
Boiling point 154 °C (lit.)
Density 0.995 g/mL at 25 °C (lit.)
Vapor Pressure 10 mm Hg ( 42.2 °C)
Refractive index n20/D 1.516(lit.)
Flash point 125 °F
Storage conditions Store at RT.
Solubility 1.71 g / l
Form Liquid
Colour Clear colorless
Odor (Odor) phenol, anise odor
Water solubility 1.6 g/L (20 ºC)
Merck 14,669
BRN 506892
Stability Stable. Flammable. Incompatible with strong oxidizing agents.
Database 100-66-3(CAS DataBase Reference)
NIST化学物质信息 Benzene, methoxy-(100-66-3)
EPA chemical substance information Anisole (100-66-3)
Toxicity GRAS(FEMA)
InChIKey RDOXTESZEPMUJZ-UHFFFAOYSA-N
Odor Threshold 0.057ppm
explosive limit 0.34-6.3%(V)
Auto-ignition temperature 887 °F

Anisole Product characteristicsand synthesis method

Product Features Anisole, also known as anisole, methoxybenzene, and methyl phenyl ether, is a colorless liquid with the odor of fennel. It has a sweet taste. It naturally exists in tarragon essential oil. It is insoluble in water and soluble inwater. Ethanol, ether and acetone are easily soluble in benzene. Irritating to eyes and mucous membranes.
It was originally obtained from distilled methyl salicylate or methoxybenzoic acid,乐动体育最新版本and now it is mainly prepared by reacting methylation reagent dimethyl sulfate with phenol in an alkaline aqueous solution.
苯甲醚是容易发生亲电取代意图ction on the aromatic nucleus. Condensed with formaldehyde to produce viscous oil or resin; reacted with phosphorus chloride to produce p-chloroanisole and a small amount of o-chlorine products; reacted with sulfuryl chloride to produce 2,4,6-trichloroanisole.
In addition, when anisole is heated with hydrobromic acid or hydroiodic acid, the carbon-oxygen bond is broken to produce phenol and methyl halide. This is an important method for determining the methoxy group on the benzene ring.
Chemical nature Colorless liquid with aromatic odor. Insoluble in water, soluble in ethanol and ether.
Production method 1. It is made by reacting methylating agent dimethyl sulfate with phenol in alkaline solution. Mix phenol with sodium hydroxide solution, and slowly add dimethyl sulfate below 10°C. After the addition is completed, the temperature is raised to 40°C and the reaction is refluxed for 18 hours, then the oil layer is separated by standing, dried with anhydrous calcium chloride and subtractive distillation to obtain anisole.
2. It is obtained by passing methyl chloride into liquid ammonia of sodium phenate and reacting. It is obtained by heating phenol and methanol together. It is derived from the reaction of phenol and dimethyl sulfate in the presence of sodium hydroxide.

What are the safety issuesofAnisole

Risk Statements 10-38-20-36/37
Hazard Codes Xn,Xi
Safety instructions 37/39-26-16-24/25
WGK Germany 2
RTECS number BZ8050000
TSCA Yes
Toxicity LD50 orally in rats: 3700 mg/kg (Taylor)
HazardClass 3

What are the safety issuesofAnisole

Raw materials Sodium hydroxide–>Dimethyl sulfate–>Phenol–>Dimethyl–>Dimethyl ether
Downstream products 1-Methyl-4-imidazolecarboxylic acid–>4-(hydroxymethyl)imidazole–>imidazole-4,5-dicarboxylic acid–>1-methyl-1H-imidazole-5-carboxylic acid–> Cefdinir–>1,5-diazabicyclo[4.3.0]non-5-ene–>1-methyl-1H-imidazole-4,5-dicarboxylic acid–>Allure Red– >Dijunjing–>Ceftibuten–>2-hydrazinomethylpyridine–>1H-imidazole-4-carboxylic acid–>Methyldopa–>1-methyl-1H-imidazole-4 ,5-Dicarbonitrile–>Pyridine-3-methylenehydrazine,1-(3-pyridyl)methylhydrazine–>Lawson’s reagent–>6-Hydroxy-1-naphthoic acid–>dispersionBlueBGL–>Bunazosin Hydrochloride–>Tracking, Trace, Trace–>M-oleamido-o-methoxybenzene sulfonate sodium, detergent MA, detergent SL–> Cefcapine pivoxil–>Verapamil–>6-Methoxynaphthoic acid–>Anoxomol Antioxidant–>Alapril–>ReactiveRedViolet KN-R–> 2-Bromoanisole–>3-(4-methoxybenzoyl)propionic acid–>4,5-dicyanoimidazole–>4-chloro-4′-hydroxybenzophenone- ->(4-Chlorophenyl)(4-methoxyphenyl)ketone–>Methoxychlor, Methoxychlor–>Anisyl acetate–>BigredLG–>2,4,6 -Tribromoanisole–>fenofibrate–>4-fluoro-4′-methoxybenzophenone

Product Storage

Keep undercool, dry and well ventilated warehouses, guard against fire.

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